硼氢化钠合成反应条件研究

Study on the Conditions of Reaction for the Synthesis of Sodium Borohydride

本文通过对由磷酸硼与金属钠在常压下固相合成硼氢化钠反应条件的研究,确定了一条能获得较高转化率的合成路线。所采用的方法,对研究同类固相反应有着普遍意义。

A new route for the synthesis of sodium borohydride is established in this paper,by studying on the conditions of reaction of boron orthophosphate with sodium in one hydrogen pressure and in dry state. High yield of sodium borohydride can be obtained by using the route presented in this paper.