摘要
氯乙酰氯用乙醇醇解转化成酯,进行气相色谱法定量分析。讨论了色谱法内标物的选择及醇解反应条件与转化率的关系,证明了氯乙酰氯在常温下很易醇解,操作简便,可实现气相色谱分析。
ChloroaceWl chloride, transformed into ester by alcoholysis with ethanol, was quantitatively analyzed by gas chromatography. The choice of internal standard compound, and effects of alcoholysis reaction condition on transformation yield were discussed., Experiments have shown that the alcoholysis of chloroacetyl chloride at room temperature is easy, the analytical procedure is convenient and the result is satisfactory.
出处
《沈阳化工学院学报》
1993年第4期283-289,共7页
Journal of Shenyang Institute of Chemical Technolgy
关键词
氯乙酰氯
醇解
气相色谱
chloroacetyl chloride
alcoholysis of acyl chloride
gas chromatography
quantitative analysis
