摘要
This paper deals with the effect of annealing on the magnetism of the sintered NdFeB magnet with a composi- tion of Nd3oB5M Alo.6Nbo.7Feft2.4- Microstructural investigations of the grain size and grain boundaries with SEM were carried out. Microstructural investigations showed the presence of some Nd-rich phase in grain boundaries and main phase. The results of magnetic properties analysis shows that this non-magnetic Nd-rich phase, produced in annealing process, can increase or decrease the magnetism of the sintered NdFeB-type permanent magnet. Appropriate amount of Nd-rich phase will strengthen the pinning field and elevated the coercive force of magnet, but too many these non-magnetism phases in Nd2Fei4B main phase will decrease it. When the sintered NdFeB magnet was annealed at 3Pa and 492°C for an hour the coercive force would raise from 915.6kA/m to 1164.8kA/m, and the (BH^ from 277.7kJ/m to 349.5kJ/m. How- ever, annealing at a non-optimized temperature at 542 °C, microstructure changes in some main phase will leading the de- crease of properties.
This paper deals with the effect of annealing on the magnetism of the sintered NdFeB magnet with a composi- tion of Nd3oB5M Alo.6Nbo.7Feft2.4- Microstructural investigations of the grain size and grain boundaries with SEM were carried out. Microstructural investigations showed the presence of some Nd-rich phase in grain boundaries and main phase. The results of magnetic properties analysis shows that this non-magnetic Nd-rich phase, produced in annealing process, can increase or decrease the magnetism of the sintered NdFeB-type permanent magnet. Appropriate amount of Nd-rich phase will strengthen the pinning field and elevated the coercive force of magnet, but too many these non-magnetism phases in Nd2Fei4B main phase will decrease it. When the sintered NdFeB magnet was annealed at 3Pa and 492°C for an hour the coercive force would raise from 915.6kA/m to 1164.8kA/m, and the (BH^ from 277.7kJ/m to 349.5kJ/m. How- ever, annealing at a non-optimized temperature at 542 °C, microstructure changes in some main phase will leading the de- crease of properties.
出处
《材料热处理学报》
EI
CAS
CSCD
北大核心
2004年第5期69-72,共4页
Transactions of Materials and Heat Treatment
基金
funded by Zhejiang Provincial Natural Science Foundation of China under Grant No.501077
关键词
永久磁铁
烧结
NDFEB
退火
磁性
permanent magnet, sintered NdFeB magnets, annealing