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Microstructure and properties of sputtered thermal barrier coatings

Microstructure and properties of sputtered thermal barrier coatings
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摘要 A 3 kW radio frequency (RF) magnetron-sputtering unit was used to producezirconia ceramic coatings on hollow turbine blades and vanes, which had been deposited a NiCrAlYbond coat layer by cathodic arc deposition. The NiCrAlY coating surface was shot-peened, and theresidual stress in the bond coat layer and the effects of heat treatment on the residual stress arepresented. After shot peening porosities and microgaps disappear in the NiCrAlY bond coat, the wholedepth profile is residual compressive stress. Coarseness tests show that the roughness value (Rz)decreases from 16.4 to 3.3 mu m. The microstructure and phase composition of the coatings wereinvestigated using electron probe microanalysis (EPMA) and X-ray diffraction (XRD). The results showthat the/ NiCrAlY bond coat is composed of gamma and Cr phases, and the A1_2O_3 scales are formednear the interface between the ZrO_2 ceramic layer and the NiCrAlY bond coat. No degradationoccurred to RF sputtered ceramic coatings after oxidating at 1150 deg C for 100 h, heating at 1150deg C for 5 min and then air-cooling for 500 thermal cycles. A 3 kW radio frequency (RF) magnetron-sputtering unit was used to producezirconia ceramic coatings on hollow turbine blades and vanes, which had been deposited a NiCrAlYbond coat layer by cathodic arc deposition. The NiCrAlY coating surface was shot-peened, and theresidual stress in the bond coat layer and the effects of heat treatment on the residual stress arepresented. After shot peening porosities and microgaps disappear in the NiCrAlY bond coat, the wholedepth profile is residual compressive stress. Coarseness tests show that the roughness value (Rz)decreases from 16.4 to 3.3 mu m. The microstructure and phase composition of the coatings wereinvestigated using electron probe microanalysis (EPMA) and X-ray diffraction (XRD). The results showthat the/ NiCrAlY bond coat is composed of gamma and Cr phases, and the A1_2O_3 scales are formednear the interface between the ZrO_2 ceramic layer and the NiCrAlY bond coat. No degradationoccurred to RF sputtered ceramic coatings after oxidating at 1150 deg C for 100 h, heating at 1150deg C for 5 min and then air-cooling for 500 thermal cycles.
出处 《Journal of University of Science and Technology Beijing》 CSCD 2004年第6期524-528,共5页 北京科技大学学报(英文版)
关键词 magnetron sputtering thermal barrier coating MICROSTRUCTURE shot peening high temperature oxidation magnetron sputtering thermal barrier coating microstructure shot peening high temperature oxidation
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参考文献1

  • 1P. D. Harmsworth,R. Stevens.Microstructure of zirconia-yttria plasma-sprayed thermal barrier coatings[J].Journal of Materials Science.1992(3)

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