摘要
研究假性紫罗兰酮在浓硫酸中环化制备β-紫罗兰酮的工艺条件。反应介质为脂肪烃或氯代脂肪烃和低级醇的混合物。β-紫罗兰酮的摩尔得率83%以上,产品中紫罗兰酮的总含量>98%,β-紫罗兰回含量>95%。
This article deals with the technological conditions for the manufacture of β─ionones by cyclitation of pseudoionones with sulfnric acid,using the mixtures of hydro carbons or chlorinated hydrocarbons and lowe alcohols as the reaction medium.The yield of β─ionones is more than83%,the concentration of ionones in product is more than 98% and β─ionones more than 95%.
出处
《福州大学学报(自然科学版)》
CAS
CSCD
1994年第1期85-88,共4页
Journal of Fuzhou University(Natural Science Edition)
关键词
环化
紫罗兰酮
香料
pseudoionones
cyclization
ionones