1，3－二氯－2－丁烯氯化产物的气相色谱分析

GAS CHROMATOGRAPHY ANALYSIS OF 1, 3-DICHLORO -2-BUTENE CHLORINATE

用气相色谱法测定１，３－二氯－２－丁烯的氯化产物，采用３０１釉化担体：阿皮松Ｌ：聚乙二醇－２０Ｍ－２－硝基对苯二甲酸＝１００：１０：０．８（质量比）的固定相填充柱分离了氯化产物中１６个组分。用色谱－质谱联用法鉴定这些组分为２，３，４－三氯－１－丁烯、２－甲基－３，３，３－三氯－１－丙烯、１，２，３，３－四氯丁烷、１，２，３，３，４－五氯丁烷等。用面积归一化法计算出了氯化产物中各组分含量。

The chlorinate of 1,3-dichloro-2-butene (DCB)was determined by gas chromatography. Sixteen components in the chlorinate were separated by a column packed with 301-glazed supporter: Apiezon-L: FFAP of 100:10:0.8 (mass ratio). The components were identified by gas chromatograph-mass spectrometer.The composition of chlorinate of DCB was determined by the area normalization method.