摘要
以三正丁胺和１－溴代正丁烷为原料，乙腈和氯仿混合液为溶剂，在一定温度下合成了相转移剂四正丁基溴化铵。产品纯度为９８．５％，产率达９２．７３％。
The method of synthesizing tetra-n-butylammonium bromide with tri-n-butylamine and 1-bromobutane as raw-material and with acetonitrile as solvent at 90～100℃ is reported。The production rate can reach 92.7% and the purity of the product is 98.51%.
出处
《河南医科大学学报》
1994年第3期251-252,共2页
Journal of Henan Medical University
关键词
三正丁胺
溴代正丁烷
溴化铵
合成
tetra-n-butylammonium bromide
tri-n-butylamine
1-bromobutane
