Tertamer有效含量测定方法

DETERMINATION OF TERTAMER BY GAS CHROMATOGRAPHIC METHOD

本文介绍Tertamer（2－溴－2－溴甲基戊二腈）气相色谱分析方法．选用7％聚丙二醇己二酸酯／ChromosorbG.AW．DMCS（80～100目）固定相，以苯酚为内标，在适宜的色谱条件下。对Tertamer进行定量分析．该方法变异系数为0.17％．回收率为98.9～101.2％．此法测定Tertamer获得个人满意结果．

a method for determincotion of 2-bromo-2-bromomethylglutaronitrile by gas. chromatograph is reviewed. The column of gas chromatograph is packed with Reoplerx 400 and Chromosorb G. AW DMES, Hydroxybenzene is used as internal standard. The relative standard diviation for the determination of 2-bromo-2-bromomethylglutaronitrile is 0. 17%.and the recoveny is thd rang of 98.9%-101.2%.The method has been applied to the determination of 2-bromo-2- bromomethylglutaronitrile in sample with satisfactory results.