摘要
探讨了从3-乙酰基酚酮出发经甲胺基化、还原、水解合成了3-(2-羟乙基)酚酮的新合成路线,使总收率从原来的20.5%提高到59.2%。所合成的化合物3为尚未见文献报道的新化合物。其结构已经红外光谱、核磁共振谱及元素分析征实.
In this paper,we studied a new route of synthesis of 3-acetyltropolone by methylamination of 3-acetyltropolone, reductipn and hydrolysis. The totalyield was 59 .2%. The structure of the new synthesized compound 3 was confirmed by elemental analysis,IR and 1HNMR spectroscopy.
出处
《化学试剂》
CAS
CSCD
北大核心
1994年第6期363-364,共2页
Chemical Reagents