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水中化学战剂水解产物的分析鉴定 被引量:1

Identification of chemical warfare agents and their hydrolysis products in water
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摘要 水中化学战剂水解产物的分析鉴定胡绪英,郭杭州,曹金鸿(军事医学科学院毒物药物研究所)【摘要】报道了水中三类代表性化学战剂水解产物的富集及检测方法。污染水样通过离子交换柱、减压浓缩、丙酮定溶,进行GC、GC/MS检测,所得质谱数据与标准品质谱数据一致。... The hydrolysis products of three types of chemical warore agents,sarin,soman,and mustard gas weredetermined by GC and GC / MS.The results showed that the chemical warfare agents(except mustard gas) andtheir hydrolysis products in contaminated water samples staying for one day can be detected.Almost all originalagents disappeared after 15 days in water while their hvdrolysis products could still be detected after as long as 3months
出处 《军事医学科学院院刊》 CSCD 北大核心 1994年第1期28-29,共2页 Bulletin of the Academy of Military Medical Sciences
关键词 化学战剂 气谱 质谱 鉴定 chemical warfare agent GC/MS
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  • 1Robin M. Black, Raymond J. Clarke, David B. Cooper, et al. Application of headspace analysis, solvent extraction,thermal desorption and gas chromatography-mass spectrompetry to the analysis of chemical warfare samples containing sulphur mustard and related compounds[J]. J Chromatogr, 1993,637: 71-80.
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  • 4Robin M. Black, Robert W. Read. Detection of trace levels of thiodiglycol in blood, plasma and urine using gas chromatography electron capture negative-ion chemical ionisation mass spectrometry[J]. J Chromatogr, 1988, 449:261-270.
  • 5Jakubowski EM, Woodard CL, Mershon MM, et al.Quantification of thiodiglycol in urine by electron ionization gas chromatography-mass spectrometry[J]. J Chromatogr,1990,528:184-190.
  • 6Mui Tiang Sng, Wei Fang Ng. In-situ derivatisation of degradation products of chemical warfare agents in water by solid phase microextraction and gas chromatographic mass spectromteric analysis[J]. J Chromatogr A, 1999,823:173-182.
  • 7D'Agostino PA, Provost LR, Hancock JR. Analysis of mustar hydrolysis products by packed capillary liquid chromatography-electrospray mass spectrometry[J]. J Chromatogr A, 1998,808:177-184.
  • 8Edwin WJ, Hooijschuur, Charles E, Kientz, Udo A. Th.Brinkman. Determination of the sulfur mustard hydrolysis product thiodiglycol by microcolumn liquid chromatography coupled on-line with sulfur flame photometric detection using large-volume injection and peak compression[J]. J Chromatogr A, 1999,849: 433-444.

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