微波辐射相转移催化合成十二烷基缩水甘油醚

Synthesis of dodecyl glycidyl ether under microwave irradiation and PTC

采用微波辐射技术,以四丁基溴化铵为相转移催化剂催化合成了十二烷基缩水甘油醚,研究了微波功率、辐射时间、反应物配比对反应产物收率的影响。实验结果表明,适当的微波辐射可以加速十二烷基缩水甘油醚的合成反应,而且产率高,操作简便。

The synthesis of dodecyl glycidyl ether was studied under microwave irradiation with TBAB as the phase transfer catalyst. Detailed studies were made on the effect of the microwave power, time of microwave radiation, and the matching of reactant on the yield ratio of reaction product. The experimental results showed that the proper microwave irradiation could speed up the reaction of dodecyl glycidyl ether and give high yield with simple operation.