摘要
目的 :对枳实生品及不同炮制品中辛弗林的含量进行考察。方法 :采用高效液相色谱法对枳实生品及不同炮制品进行定量分析 ,色谱柱为C18,流动相为甲醇 -水 (43∶57),检测波长为275nm,柱温为40℃,流速为1 0ml/min。结果 :辛弗林的含量以醋炙品为最高 ,酒炙品为最低。结论 :枳实不同炮制品的内在质量有明显差异。
OBJECTIVE:To explore the contents of synephrine in raw Fructus Aurantii Immaturus and its processed products.METHODS:HPLC was used for the quantitative analysis of raw Fructus Aurantii Immaturus and its processed products;C 18 was used as the Chromatographic column;methanol-water(43∶57)which contained0.1%phosphoric acid and0.1%soldium dodecyl sulfonate was used as the mobile phase with a detected wavelength at275nm,column temperature at40℃and a flow speed at1.0ml/min.RESULTS:Synephrine contents of the vinegar-fried product was the highest and that of the alcohol-fried product was the lowest.CONCLUSION:There is a significant difference in intrinsic quality among various processed products of Fructus Aurantii Immaturus.
出处
《中国药房》
CAS
CSCD
北大核心
2005年第5期395-397,共3页
China Pharmacy
关键词
枳实
炮制品
辛弗林
高效液相色谱法
含量
Fructus Aurantii Immaturus
Processed product
Synephrine
HPLC
Contents
