过氧多酸研究──Ⅱ．K_（12）H_2［W（OH）_5（H_2O）（VO（O_2）2－OH－VO（O_2）_2）_5］·2H_2O的合成及表征

STUDIES ON PEROXOPOLYOXOMETALATES Ⅱ. SYNTHESIS AND CHARACTERIZATION OF K_(12)H_2[W(OH)_5(H_2O)(VO(O_2)_2)-OH-VO(O_2)_2)_5]·2H2O

过氧多酸研究──Ⅱ．Ｋ_（１２）Ｈ_２［Ｗ（ＯＨ）_５（Ｈ_２Ｏ）（ＶＯ（Ｏ_２）２－ＯＨ－ＶＯ（Ｏ_２）_２）_５］·２Ｈ_２Ｏ的合成及表征张权，岳斌，朱思三，金松林，谢高阳（复旦大学化学系，上海２００４３３）关键词白钨酸，过氧化氢，μ－氧·二［二过氧根·?..

The mixed metal peroxide, K(12)H2[W(OH)5(H2O)(VO(O2)2-OH-VO(O2)2)5]·2H2O, was obtained from the reaction of WPTA, KVO3 and H2O2. This compound was characterized by elemental analysis,IR spectra, DTA-TG thermal analysis and UV spectra.Its structure was also suggested.