摘要
An innovative photoelectrode, B 2O 3·TiO 2/Ti electrode, was prepared by galvanostaticanodisation. The morphology and crystalline texture of the B 2O 3·TiO 2 film on electrode were examined by atomic force microscopy(AFM) and X-ray diffraction respectively. The examination results indicated that the anatase was the dominant component. The kinetics of photoelectrocatalytic(PEC) degradation of humic acid(HA) was investigated; the results demonstrated that effects from strongness to weakness on the photoelectrocatalytic degraded rate of humic acid: power of UV-lamp, area of TiO 2 film, bias, original concentration of humic acid solution. The optimum conditions were power of UV-lamp 125 W, area of TiO 2 film 42.0 cm 2, bias 1.4 V, original concentration of humic acid solution 5 mg/L in this PEC reaction system.
An innovative photoelectrode, B 2O 3·TiO 2/Ti electrode, was prepared by galvanostaticanodisation. The morphology and crystalline texture of the B 2O 3·TiO 2 film on electrode were examined by atomic force microscopy(AFM) and X-ray diffraction respectively. The examination results indicated that the anatase was the dominant component. The kinetics of photoelectrocatalytic(PEC) degradation of humic acid(HA) was investigated; the results demonstrated that effects from strongness to weakness on the photoelectrocatalytic degraded rate of humic acid: power of UV-lamp, area of TiO 2 film, bias, original concentration of humic acid solution. The optimum conditions were power of UV-lamp 125 W, area of TiO 2 film 42.0 cm 2, bias 1.4 V, original concentration of humic acid solution 5 mg/L in this PEC reaction system.
基金
TheScientificResearchFoundationofHarbinInstituteofTechnology(No.HIT .2 0 0 1 56)