摘要
选择四甲基四氢环四硅氧烷作模型化合物,利用Si-H伸缩振动在216Ocm ̄(-1),的吸收作定量分析峰,以红外光谱法测定含氢硅油和烯丙基醚加成产物中残留Si-H的含量,所得结果与化学法测定结果一致。
In this paper a new way for the determination of Si-H groups content in the addition product of hy-drogen polysiloxane fluid and allyl-ether by means of IR was described,selecting tere-methyl tere-hydrogencyclosilicone as model compound and Si-H stretching vibration(2 1 60cm ̄(-1))as qualitative analysis absorp-tion bands.The results showed there was no difference with that of chemical analysis.