摘要
以木素磺酸钙为原料,利用反相悬浮聚合技术制备出球状木素基离子交换树脂。研究了分散相、分散剂、聚合温度、搅拌条件及交联剂用量等对悬浮聚合反应及成球效果的影响,并对产品的外观、粒度、含水量、密度及交换容量等基本性能进行了表征和测定。在优化条件下制得的球形木素基离子交换树脂的交换容量可达3.83mmol/g。
A spherical lignin-based ion exchange resin was prepared with calciumlignosulfonate as raw material in a cheap and non-toxic disperse phase by reversed phase suspension polymerization technique. The effect of disperse phase, dispersing agent and cross-linking agent dosage, polymerization temperature and mixing speed on the suspension polymerization and sphericization were studied in detail. The fundamental performances of the resin including appearance, particle size, moisture content, density, and exchange capacity were characterized. At the optimal conditions, the ion exchange capacity of 3.83 mmol/L was reached.
出处
《中国造纸》
CAS
北大核心
2005年第5期18-22,共5页
China Pulp & Paper
关键词
木素磺酸钙
反相悬浮聚合
离子交换树脂
基本性能
calciumlignosulfonate
reversed phase suspension polymerization
ion exchange resin
fundamental characteristics