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1,3-二溴丙酮与苯基硫脲的反应研究 被引量:4

Study on the reaction of 1,3-dibromoaetone with phenyl thiourea
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摘要 1,3-二溴丙酮和苯基硫脲反应生成4-溴甲基-2-苯甲酰基亚胺基-3-苯基噻唑啉,产物结构经红外光谱、核磁共振光谱和质谱表征. 4-Bromomethy-2-benzoylimino-3-phenyl thiazoline was prepared by the reaction of 1,3-dibromoacetone with phenyl thiourea,its structure was characterized by IR,NMR and MS spectra.
出处 《苏州大学学报(自然科学版)》 CAS 2005年第2期68-69,72,共3页 Journal of Soochow University(Natural Science Edition)
基金 江苏省有机合成重点实验室资助项目(JSK016)
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  • 1MARCANTONIO K M,CHEN C Y.Apractical preparation of 5-(ketoaryl)thiazoles[J].Tetrahedron Letters,2002,43:8845-8848.
  • 2TAYLOR R E,HALEY J D.Towards the synthesis of epothilone A:enantioselective preparation of the thiazole sidechain and macrocyclic ring closure[J].Tetrahedron Letters,1997,38:2061-2064.
  • 3GOFF D,FEMANDEZ J.The preparation of 2,4-disubstituted thiazoles on solid support[J].Tetrahedron Letters,1999,40:423-426.
  • 4MENGER F M,PERSICHETTIR R A.Two new amphiphilic catalysts for ester hydrolysis[J].J Org Chem,1987,52:3451-3452.

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