摘要
合成了双(5-磺酸钠水杨醛)丙酰二肼席夫碱及其Cu( ),Ni( ),Zn( ),Mn( ),Co( )的配合物,用元素分析、IR、摩尔电导和电子光谱对所得化合物进行了表征,对席夫碱配体还进行了1HNMR和MS表征,对所合成化合物的组成和结构进行了分析.
<Abstrcat> The Schiff base of propanedioyl dihydrazide with sodium salicylaldimine-5-sulphonate and its Cu(Ⅱ),Ni(Ⅱ),Zn(Ⅱ),Mn(Ⅱ),Co(Ⅱ)complexes have been synthesized. These compounds have been characterized by elemental analysis,IR,molar conductivity and electronic absorption spectrum. The Schiff base ligand has been further characterized by ()~1H NMR and MS. The coordination composition and structure in these compounds are also analysed.
出处
《华中师范大学学报(自然科学版)》
CAS
CSCD
2005年第2期208-211,共4页
Journal of Central China Normal University:Natural Sciences
基金
湖北省自然科学基金资助项目(98J048).
关键词
丙酰二肼
水溶性席夫碱
配合物
propanedioyl dihydrazide
water-soluble Schiff base
complex