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热解吸──气相色谱法测定气相样品中的苯系物

Analysis of Alkyl Benzenes in Gaseous Samples by Thermal Desorption-Gas Chromatography
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摘要 采用装有GDX-102的采样管,直接常温吸附大气和石油化工排放废气中的苯系物,然后以加热解析──气相色谱法测定。以苯、甲苯、乙苯、对二甲苯、间二甲苯、邻二甲苯、苯乙烯等七种苯系物为研究对象,确定了采样──分析的最佳操作条件。本方法具有操作简单,能准确测定污染成分等优点,平均回收率可达81.5%,变异系数小于7.8%。在采集1L气体样品时,相应采样速度200mL/min,对七种苯系物的最低检测限可达ppb级。 A method for the determination of benzene and its c≤c8 derivative in gaseous samples which were absorbed with GDx-102 at ambient temperature by thermal desorption-gas chromatography is introduced. The optimum sampling analytical conditions were found by using seven(C6-C8) alkyl benzenes as the studied objects. The method has the following advantages: the operation procedure is simple, the average recovery is 81.59%, the relative standard deriation is less than 7.8% and minimun of determination is ppb level.
作者 王波 曾向东
出处 《石油化工环境保护》 1994年第1期50-51,共2页 Environment Protection in Petrochemical Industry
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