摘要
本文采用两步缩合,先以二硝基氯苯(代替苦基氯)与2,6-二氨基吡啶反应得到N-(2,4-二硝基苯基)-2,6-二氨基吡啶(2),(2)再与苦基氯缩合得到N-(2,4-二硝基苯基)-N'-苦基-2,6-二氨基吡啶(3),将(3)硝化就得到题称化合物(4)。
This paper reports a new method of synthesizing 2,6-bis(picrylamino)-3,5-dinitropyridine by condensation reaction of 2,6-diaminopyridine and 2,4-dinitro-chlorobenzene the condensation product was then reacted with picrylchloride and getN-(2,4-dinitrophenyl)-N '-picry1-2,6-diaminopyridine(3) which was nitrated and ob-tained the titled compound(4).
出处
《含能材料》
EI
CAS
CSCD
1994年第3期25-28,共4页
Chinese Journal of Energetic Materials