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盐酸氟奋乃静片含量均匀度的流动注射分析 被引量:2

FLOW-INJECTION ANALYSIS OF CONTENT UNIFORMITY OF FLUPHENAZINE HYDROCHLORIDE
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摘要 基干盐酸氟奋乃静在一定pH值下与氯化钯反应,生成红色配位产物,于485nm处出现最大吸收,可籍以测定含量。线性范围0~80μg/ml,RSD约为1%。 A spectrophotometry of the content uniformity of fluphenazine hydrochloride (1) in a flow-injection analysis system was based on the color-reaction of 1 with palladium chloride, measured at 485nm. The calibration curve was linear from 0 to 80μg/ml, the RSD was about 1%.
出处 《中国医药工业杂志》 CAS CSCD 北大核心 1995年第6期266-268,共3页 Chinese Journal of Pharmaceuticals
关键词 流动注射分析 盐酸氟奋乃静 含量均匀度 flow-injection analysis, fluphenazine hydrochloride, content uniformity, spectrophotometry
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参考文献1

  • 1安登魁.药物分析[M]人民卫生出版社,1998.

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  • 1翟屹民,秦英绂,徐敏洁,李文标,郭桂欣.高效液相色谱法测定血浆中常用精神病治疗药物[J].中国医院药学杂志,1997,17(4):159-161. 被引量:12
  • 2Ortiz SL , Gomez BC, Martinez CJ. Determination of fluphenazine hydrochloride in a flow assembly incorporating cerium(Ⅳ)arsenite as a solid-bed sector [J]. Analytica Chimica Acta, 1993, 276 (2) : 281 - 286.
  • 3EL-ragehyNA, AbbasSS, EL- khateebSZ. Spectrophotometric and stability indicating high performance liquid chromatographic determination of nortriptyline hydrochloride and fluphenazine hydrochloride [J]. Anal Lett., 2002, 35(7): 1171-1191.
  • 4Wenbing S, Jidong Y, Yuming H. Ion-pair complexbased solvent extraction combined with chemiluminescence determination of chlorpromazine hydrochloride with lurninol in reverse mieelles [J]. J Pharmaeeut Biorned, 2004, 36(1): 197-203.
  • 5Fujiwara T, Mohammadzai IU, Murayama K, et al. Solvent extraction coupled on-line to a reversed micellar mediated chemiluminescence detection system for trace-level determination of atropine [J]. Anal Chem, 2000, 72(7): 1715-1719.
  • 6Imdadullah , Fujiwara T , Kumamaru T . Solvent extraction and chemiluminescence determination of gold in silver alloy with luminol in reverse micelles [J]. Anal Chem, 1993, 65(4): 421-424.
  • 7国家药典委员会.中华人民共和国药典[M].北京:化学工业出版社,2000.168.
  • 8中华人民共和国药典委员会.中国药典(二部)[M].附录Ⅷ.北京:化学工业出版社,2005:54-57.
  • 9王亦平.吩噻嗪类药物制剂的流动注射分析测定[J].中国医药工业杂志,1999,30(3):133-134. 被引量:2
  • 10张兰,陈国南,方禹之.毛细管电泳-柱端安培检测装置的研制[J].福州大学学报(自然科学版),2000,28(6):85-88. 被引量:4

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