摘要
用发烟硫酸氧化2乙基1硝基蒽醌合成了蒽醌〔1,2-C〕甲基异噁唑,通过质谱、核磁共振对蒽醌〔1,2-C〕甲基异噁唑结构进行了表征,并给出了蒽醌〔1,2-C〕甲基异噁唑较优的合成条件及薄层色谱分离条件。
Anthraquinone〔1,2-C〕methylisoxazole was prepared from 2-ethyl-1-nitro- anthraquinone through oxidation by oleum. The structure of obtained title compound was characterized by 1H NMR and MS. The optimum synthesis conditions and separation conditions for TLC were given in this paper.
出处
《精细与专用化学品》
CAS
2005年第13期21-23,共3页
Fine and Specialty Chemicals
