摘要
以氯乙酸、异丙醇直接酯化制备氯乙酸异丙酯,使用Fe2(SO4)3·xF2O催化可简化产品后处理操作.得酯收率83.8%.
Isopropyl chloroacetate synthesized by using Fe2 (SO4 )3·xH2O as catalyst. The products can be directly separated by distillation without washing and neutralization. The yield was 83. 8%.
关键词
异丙醇
氯乙酸异丙酯
硫酸铁
催化法
合成
chloroacetic acid isopropyl alcohol isopropyl chloroacetate ferric sulfate catalysis