摘要
海水样品用乙酸乙酯萃取后,萃取液加入乙酸和氧化铬,在100℃下回流30min,再用正己烷萃取,干燥、浓缩、定容后进行色谱测定。方法简便易行,准确度高。该法已用于青岛胶州湾海水中有机氯农药残留量的测定进行验证。
In this Paper, a rapid and precise determination of chlorinated pesticides in seawaterby gas chromatography is reported.0.5 liter of seawater was extraeted with ethyl ac-etate. acid hydrolysis and followed by extraction with n-hexane and electron caputuredetector gas chromatography.The precedure described in this paper is a convenient andreliable method lor the determmation of BHC and DDT of BHC and DDT from 0. 5liter sample of seawater. Experimental result, Compared with Common analysis, wassatisfactory.
出处
《海岸工程》
北大核心
1995年第1期18-22,共5页
Coastal Engineering