摘要
介绍了甲烷磺酰氯的几种合成方法。探讨了反应温度、通氯速度、氯气用量、盐酸浓度和用量对产品收率及质量的影响，确定了适宜的工艺条件。介绍了粗品精制的过程。
Processes for synthesis of methanesulfonyl chloride are described.Effect of reaction temperature, chlorine feed rate, consumption of chlorine,consumption and concentration of hydrochloric acid, on the product yield andquality,is discussed,suitable process conditions are determined. Purificationof the raw product is described, too.
出处
《河北化工》
1995年第3期5-7,共3页
Hebei Chemical Industry
关键词
甲烷磺酰氯
合成
精制
甲硫醇
二甲基二硫
methanesulfonyl chloride,synthesis, purification,dimethylthiocarbonate thiourea,dimethyl sulfate, methanthiol,methyl disulfide
