摘要
用减压蒸馏装置代替克达尔定氮法的水蒸汽蒸馏装置,仪器简单、操作方便、驱氨完全迅速.氨回收率为99.49%~100.08%,方法重现性好,相对标准偏差为0.02,变异系数为0.25%.
Steam Distillation in Kjedahl Method for Determining Nitrogen is replaced by vacuum distillation.The apparatus and operation was simple,ammonia was completely and rapidly transfered with the improved method.The relative standard deviant was 0.02,and the coefficient of variation was 0.25%.The recovery rate was between 99.49%and 100.08%.