期刊文献+

克达尔定氮法的改进 被引量:1

Improvement of Kjedahl Method for Determining Nitrogen
原文传递
导出
摘要 用减压蒸馏装置代替克达尔定氮法的水蒸汽蒸馏装置,仪器简单、操作方便、驱氨完全迅速.氨回收率为99.49%~100.08%,方法重现性好,相对标准偏差为0.02,变异系数为0.25%. Steam Distillation in Kjedahl Method for Determining Nitrogen is replaced by vacuum distillation.The apparatus and operation was simple,ammonia was completely and rapidly transfered with the improved method.The relative standard deviant was 0.02,and the coefficient of variation was 0.25%.The recovery rate was between 99.49%and 100.08%.
出处 《湖北医科大学学报》 1995年第4期301-302,共2页
关键词 克达尔定氮法 nitrogen/AN,methods
  • 相关文献

同被引文献21

  • 1王孝杰,孙建平,李效东,刘克良.氨基化单甲氧基聚乙二醇的合成研究[J].精细化工中间体,2006,36(1):40-42. 被引量:15
  • 2Carmen M B. Perspective Articles on the utility and application of solution phase combinatorial chemistry[J]. J Comb Chem, 2000, 2(2): 89--103.
  • 3Antony C, Philip B, David F, et al. Amino-derivatised beaded cellulose gels. Novel accessible and biodegradable scavenger resins for solution phase combinatorial synthesis [J]. Gre Chem,2000,2(2) : 57--62.
  • 4Cara E H, Morag A M E, Jason P T, et a l. Solid-supported cyclohexane-1,3-dione (CHD):A" capture and release"reagent for thesynthesis of amides and novel scavenger resin[J]. Org Lett,2003,5(6): 849--852.
  • 5Lindsley C W, Zhao ZJ, Leister W H. Fluoro-tethered quenching reagents for solution phase parallel synthesis [J]. Tetrahedron Lett, 2002, 43(23): 4225--4228.
  • 6Noha G, Jean M, Didier S. A new high--loading watersoluble scavenger for anhydrides, acid chlorides and isocyanates [J]. Tetrahedron Lett, 2002, 43: 1693-1695.
  • 7Moore J D, Herpel R H, Lichtsin J R, et al. ROMP-generated oligomeric sulfonyl chlorides as versatile soluble scavenging agents[J]. Org Lett, 2003, 5(2): 105--107.
  • 8Song GH, Cai YQ, PengY Q. Amino-functionalized ionic liquid as a nucleophi-lie scavenger in Solution Phase Combinatorial Synthesis[J]. J Comb Chem, 2005, 7: 561--566.
  • 9Booth R J, Hodges J C. Polymer-supported quenching reagents for parallel purification [J]. J Am Chem Soc, 1997, 119(21) : 4885--4886.
  • 10Chen J. Protocols for amide high speed analoging preparation of novel, small molecules cathepsin Dinhibitors [J]. Tetrahedron Lett, 1999, 40(52): 9195--9199.

引证文献1

二级引证文献1

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部