α-(对硝基苯氧基)十四酸酰肼的合成

Synthesis of α-(p-nitrophenoxy)myristyl hydrazide

报道了α-(对硝基苯氧基)十四酸酰肼的合成方法。以十四酸为原料经α-(对硝基苯氧基)十四酸乙酯中间体,用水合肼肼解得到α-(对硝基苯氧基)十四酸酰肼。用乙腈-氯仿混合溶剂重结晶获得纯品,收率67.9%。通过元素分析、红外光谱及核磁共振谱确定了该化合物的结构。

Synthesis of α-（p-nitrophenoxy） myristyl hydrazide from myristic acid was reported. It was prepared by reaction of ethyl α-（p-nitrophenoxy ）myristate with hydrazine hydrate, which was recrystallized with acetonitrile-trichloromethane,the yield of the product is 67.9%. The structure of the title compound is characterized by elemental analysis,IR and ^1 H NMR spectra.