摘要
金属锡为阳极，阴极为钛网，电解温度为７０℃，槽电压为６．５Ｖ，电解９０ｍｉｎ，电流效率为６９．１％，与异辛酸的转化率为９８．６％，异辛酸亚锡产率为９５．２％，耗电量为１．２０ｋ·ｈ／ｋｇ。
Abstract The synthesis of high-purity tin(Ⅱ)2-ethylhexanoate by electrochemical process fromtin and 2-ethylhexanoic acid was studied usingtin as anode.Thebest results were obtainedwith titanium net as cathode,BHT and BPS asantioxidant, at 70℃,cell voltage being 6.5V.Under these conditions, tin conversion was 98.6%, current emciencv was 69.1%,the yield of TEH was 95.2%, the power consumption ofTEH was 1. 20kW·h/kg.
出处
《精细化工》
CAS
CSCD
1995年第3期64-66,共3页
Fine Chemicals
