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当归补血汤汤剂中挥发油成分的GC-MS分析 被引量:8

GC-MS analysis of volatile oil of Danggui Buxue Decoction
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摘要 目的:探讨当归补血汤汤剂(黄芪、当归)中挥发油的主要成分。方法:采用GCMS方法分析挥发油主要组分。在进样口温度250℃,接口温度230℃,载气流速1.3mL·min-1,柱压为100kPa,升温速率3℃·min-1的色谱条件下,挥发油主成分可达到较好分离。结果:当归补血汤汤剂中挥发油的主要成分为反式藁本内酯、正丁烯基苯酞、正丁基苯酞、顺式藁本内酯等。结论:当归补血汤汤剂中挥发油成分主要来自当归挥发油成分。 AIM : To study the main components of volatile oil of Danggui Buxue Decoction ( Radix Astragali Radix Angelicae Sinensis) . METHODS : The main components of volatile oil were determined by GC-MS. The injector temperature was 250℃. The interface temperature was 230℃. The column flow was 1.3 mL ·min^- 1. The column pressure was 100 kPa. The temperature rate was 3℃·min^-1. RESULTS: The main components of volatile oil of Danggui Buxue Decoction were composed of trans-ligustilide, butylidene phthalide, n-butylphthalide, and cis-ligustilide. CONCLUSION: The main components of volatile oil of Danggui Buxue Decoction come mainly from volatile oil of Radix Angelicae sinensis.
出处 《中成药》 CAS CSCD 北大核心 2005年第8期892-894,共3页 Chinese Traditional Patent Medicine
基金 广东省中医药管理局资助课题(103025)
关键词 当归补血汤 挥发油 GC-MS Danggui Buxue Decoction volatile oil GC-MS
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