摘要
依据锑(Ⅲ)对铬(Ⅵ)─碘化钾氧化还原反应的诱导效应,建立了测定微量锑的诱导动力学光度法。本法测定锑(Ⅲ)的线性范围为0~3.0μg/mL,检测限为0.005μg/mL。测定锡合金中锑含量,结果满意。
A kinetic spectrophotometric method for determination of antimony had been proposed based on the inductive effect of antimony(Ⅲ) on the chromium(VI)-iodide redox reaction. The calibration graph is linear for 9 ̄3.Oμg/mL Sb (Ⅲ), and the detection limit is 0.005μg/mL.The content of antimony in the tin based alloy had been determined with the proposed method. The results are satisfactory.
出处
《烟台师范学院学报(自然科学版)》
1995年第3期45-48,共4页
Yantai Teachers University journal(Natural Science Edition)