摘要
采用硅胶柱色谱与配位体交换薄层色谱（ＰｄＣｌ２／ＳｉＯ２）两步分离，从煤的索氏抽出物芳烃馏分中分离出含硫多环芳香化合物（ＰＡＳＨ）和其他芳香组分，并用毛细管气相色谱（ＦＩＤ和ＦＰＤ）与色质联用仪分析了它门的组成结构。
Polynuclear aromatic sulphur heterocycles(PASHs)and other polynuclear aromatic compounds are isolated from a coal Soxhlet extract by two-step separation method using silica gel column chromatography and ligand exchange thin layer chromatography(PdCl2/SiO2).The subfractions are examined by capillary column gas chromatography with flame ionization detector and flame photometric detector and gas chromatography-mass spectrometry.
出处
《烟台师范学院学报（自然科学版）》
1995年第4期52-55,共4页
Yantai Teachers University journal(Natural Science Edition)
关键词
煤
抽出物
硫化合物
气相色谱
索氏抽出物
分离
coal extract,sulphur heterocycles,ligand exchange chromatography,GC,GC/MS
