摘要
报道了2,5-二氯-4-溴苯酚的合成工艺。对二氯苯经溴化、水解得该产物。本文提出了新的催化剂、水解反应性溶剂和导水剂,从而建立了常压法水解新工艺,缩短了反应时间,提高了合成反应的安全性,为该中间体的工业化生产提供了实验依据。
The synthesis of 2, 5-dichloro-4-bromophenol was studied. After the bromination of pdichlorobennzene and then its hydrolyzation the final product was prepared. Owing to use the better catalyst, new hydrolytic reaction solvent and the leading water agent, the new tehnology of normal pressure was established. In the new technology,the reaction time was reduced, the safety of operation was raised.
出处
《浙江工业大学学报》
CAS
1995年第2期147-152,共6页
Journal of Zhejiang University of Technology
关键词
二氯溴苯酚
合成
杀虫剂
中间体
Dichloro-4-Bromophenol
General
Pussure method
Reaction solvent