摘要
以自制的硫酸氢钠为催化剂,以冰乙酸与异丙醇为原料合成了乙酸异丙酯。最佳反应条件为:以0.2摩尔异丙醇为基准,醇酸摩尔比为1:1.5,催化剂用量为1.2g,反应温度控制在回流温度。酯收率最高可达到75.2%。
Isopropyl acetate, was synthesized using sodium bisulfate made by ourselves as catalyst, with acetic acid and Isopropyl as materials. The best condition of reaction is： if, on the basis of 0.2mol isopropyl, the mass of catalyst reaching 1.3g, the temperature of reaction controlled about 95, the rate of isopropyl and acetic acid is 1 to 1.5, the highest yield of the reaction can reach75.2%.
