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Pb-Sn-Cd三元合金纳米微粒的制备与表征 被引量:1

Preparation and characterization of ternary Pb-Sn-Cd all oy nanoparticles
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摘要 Ternary Pb-Sn-Cd alloy nanoparticles were prepared b y the sonochemical dispersion method. The nanoparticles were found to be about 40 —60 nm and coated with an amorphous layer of surfactant dioctadecyldithiophosph ate(DDP).The formation and constituent of the as-prepared nanoalloy were charac terized by transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), X-ray diffraction (XRD), differential thermal anal ysis and thermogravimetry (DTA-TG), and Fourier transform infrared (FT-IR) spe ctrophotometer.It was also found that the powder showed excellent antiwear prope rty by tribological test results. Ternary Pb-Sn-Cd alloy nanoparticles were prepared by the sonochemical dispersion method. The nanoparticles were found to be about 40--60 nm and coated with an amorphous layer of surfactant dioctadecyldithiophosphate (DDP). The formation and constituent of the as-prepared nanoalloy were characterized by transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), X-ray diffraction (XRD), differential thermal analysis and thermogravimetry (DTA-TG), and Fourier transform infrared (FT-IR) spectrophotometer. It was also found that the powder showed excellent antiwear property by tribological test results.
出处 《化工学报》 EI CAS CSCD 北大核心 2005年第8期1590-1593,共4页 CIESC Journal
基金 国家高技术研究发展计划基金项目(2002AA302607)~~
关键词 Pb—Sn-Cd三元合金 纳米微粒 超声分散 Pb-Sn-Cd ternary alloys nanoparticle sonochemical dispersion
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