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伊拉地平中有机溶剂残留量的毛细管GC测定 被引量:2

Determination of Residual Organic Solvents in Isradipine by Capillary GC
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摘要 A capillary GC method for the determination of residual solvents——ethanol, ethyl acetate and toluene in isradipine was established. A ZB-624 capillary column was used. The calibration curves were linear in the ranges of 30 - 600, 30 - 600, 10 - 150μg/ml, respectively. The average recoveries were 100.2%, 99.3% and 97.5%, respectively. A capillary GC method for the determination of residual solvents ethanol, ethyl acetate and toluene in isradipine was established. A ZB-624 capillary column was used. The calibration curves were linear in the ranges of 30-600, 30-600, 10-150μg/ml, respectively. The average recoveries were 100.2%, 99.3% and 97.5%, respectively.
出处 《中国医药工业杂志》 CAS CSCD 北大核心 2005年第9期574-575,共2页 Chinese Journal of Pharmaceuticals
关键词 有机溶剂残留量 毛细管气相色谱法 地平 测定 GC 钙离子拮抗剂 不良反应 合成过程 乙酸乙酯 isradipine residual organic solvent capillary GC determination
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