摘要
采用一步法首次合成了N,N'-二安替比林-1,6-己二酰胺(BAPHDCA),通过元素分析,UV、IR光谱和1HNMR谱分析对其结构组成进行了确认和表征,并考察了它在几种常见溶剂中的溶解性。
N, N'-Bis (antipyrine-4'-yl)-1, 6-hexanedicarboxamide as one kind of N, N'-bis (antipyrine-4'-yl)dicarboxamide has been synthesized in good yield by reacting the corresponding acid halide (hexanedioyl chloride) with 4-aminoantipyrine in benzene. The product was characterized by elemental analysis, IR, UV and 1HNMR spectra, and its solubilities in some common solvents have been tested.
出处
《化学试剂》
CAS
CSCD
北大核心
1996年第1期37-38,共2页
Chemical Reagents
关键词
二安替比林
己二酰胺
氨基安替比林
溶解性
N,N'-bis (antipyrine-4'-yl)-1, 6-hexanedicarboxamide,4-aminoantipyrine, synthesis