肤阴洁复方黄松洗液的GC-MS分析

Determination of Fuyinjie Compound Huangsong Lotion by GC-MS

目的采用GCMS法分析肤阴洁复方黄松洗液(黄松、岗柏、满山香等)的成分。方法采用HP5MS弹性石英毛细管柱,程序升温,以EI离子源和四极杆质量分析器进行分析,质谱图用NIST98谱库检索,结合人工谱图解析,鉴定各种成分,并用色谱峰面积归一化法测定其相对百分含量。结果分离出39个色谱峰,鉴定出31种成分,占已分离组分总含量的90以上。其中4松油醇、α石竹烯、β石竹烯、芳樟醇和桉油精是其中所含的相对含量较高的成分。结论该法简便、快速、灵敏度高。

AIM ： To analyze the chemical composition and their relative contents of Fuyinjie Compound Huangsong Lotion. METHODS： A capillary column HP-5 MS was used. The column temperature was controlled by a program and the MS analysis was performed with EI and quadrupole mass analyzer. The chemical composition was identified by NIST98 searching and mass spectra comparing, and their relative contents were determined by using normalization method of chromatographic peak areas. RESULTS： There were 39 components found and 31 composed of more than 90% separated components were identified. CONCLUSION： The GC-MS is a simple, rapid and sensitive method for the chemical composition analysis of Fuyinjie Compound Huangsong Lotion.