摘要
1-Chloro-3-(2′-ethoxyethoxy)-propane was prepared from 3-chloro-propanol and ethoxy-ethene with dichloroacetic acid as the catalyst and a yield of 96.2%.3-(2′-Ethoxyethoxy)propyl lithium was(then) synthesised from 1-chloro-3-(2′-ethoxyethoxy)-propane and lithium-sodium alloy in a high yield(86%) in a high vacuum reactor.It can be used as an anion polymerization initiator.
1-Chloro-3-（2′-ethoxyethoxy）-propane was prepared from 3-chloro-propanol and ethoxy-ethene with dichloroacetic acid as the catalyst and a yield of 96.2%. 3-（2′-Ethoxyethoxy）propyl lithium was then synthesised from 1-chloro-3-（2′-ethoxyethoxy）-propane and lithium-sodium alloy in a high yield（ 86% ） in a high vacuum reactor. It can be used as an anion polymerization initiator.
出处
《应用化学》
CAS
CSCD
北大核心
2005年第10期1149-1151,共3页
Chinese Journal of Applied Chemistry
基金
国家自然科学基金(20376070)资助项目
