摘要
目的:测定莲芩胶囊中黄芩苷的含量。方法:采用高效液相色谱法,以ODSC18为色谱柱,甲醇-水-磷酸(45:55: 0.21)为流动相,检测波长为280 nm。结果:黄芩苷在0.08-4.0μg线性关系良好(r=0.999 8)。平均回收率98.9%,RSD= 2.0%。结论:本方法测定简便、快速,测定结果准确。
Objective: To determine the content of baicalin in lianqin capsules. Method: HPLC method was used. The stationary phase was ODS column and the mobile phase was methanol-water-phosphoric acid (45: 55:0.21 ). The detection wavelength was 280 nm. Result: There was good linear relationship within the range of 0.08-4.0 μg for baicalin (r = 0. 999 8). The average recovery was 98.93% (RSD = 2.00% ). Conclusion: This method is simple, fast and accurate.
出处
《中国药师》
CAS
2005年第10期823-824,共2页
China Pharmacist