摘要
本文给出了金刚烷及其异构体合成物系毛细管气相色谱及色谱-质谱联用分析方法。色谱柱为CBP1键合石英毛细管、氢火焰检则器。列出了标准曲线和检测条件,回收率为98.3%~101.2%,相对标准偏差<4.0%。本方法定量分析快速、简便、准确。
This paper describes a capillary GC and GC-MS analytical method for the synthet ic adamantane and its isomers. The procedure involves the use of a fused silica column filled with bonded CBP1 stationary phase and FID detector. Standard curves and detection condi tions are given. The recoveries are 98. 3%~ 101. 2%. The RSD is less than 4. 0%. This quantitative analysis is fast, simple and accurate.
出处
《分析化学》
SCIE
EI
CAS
CSCD
北大核心
1996年第3期337-340,共4页
Chinese Journal of Analytical Chemistry
关键词
金刚烷
气相色谱
四氢双环戊二烯
色谱
质谱
Adamantane, capillary gas chromatography, tetrahydrodicyclopentadiene, gas chromatography-mass spectrometry