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氧化锌棒晶的热液制备与表征 被引量：2

Hydrothermal Synthesis and Characterization of ZnO Rod-Like Crystal
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摘要 以二水醋酸锌、氢氧化钠为原料,长链聚乙二醇(PEG-20000)、环己烷为添加剂,制备出氧化锌微晶粉体.采用X射线衍射,扫描电镜和透射电镜等分析手段对粉体进行了表征.实验结果表明,在热液环境中,利用长链PEG不仅可以制备特殊形貌的氧化锌,也可以在环己烷的作用下,制备出大长径比的一维氧化锌棒. Zn（Ac）2·2HaO and NaOH were used as experimental material to synthesize ZnO microcrystal powder with longchain PEG and cyclohexane as additives. XRD, SEM and TEM were used to characterize the powder. The experimental results showed that not only the special shape of ZnO was produced under the action of long-chain PEG, but also the one-dimension of rod-like ZnO with big aspect ratio can also be produced under the action of cyclohexane.
作者 张艳辉 田彦文 邵忠财 钱建华
机构地区 东北大学材料与冶金学院 沈阳理工大学环境与化学工程学院 渤海大学化学化工学院
出处 《东北大学学报（自然科学版）》 EI CAS CSCD 北大核心 2005年第11期1096-1098,共3页 Journal of Northeastern University(Natural Science)
基金 国家自然科学基金资助项目(50174015)
关键词 氧化锌 棒晶 PEG 环己烷 水热法 ZnO rod-like crystal PEG cyclohexane hydrothermal synthesis
分类号 O782.2 [理学—晶体学]
  • 相关文献

参考文献10

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共引文献20

同被引文献15

  • 1陶新永,张孝彬,孔凡志,林森,程继鹏,黄宛真,李昱,刘芙,许国良.PEG辅助氧化锌纳米棒的水热法制备[J].化学学报,2004,62(17):1658-1662. 被引量：36
  • 2张跃,袁洪涛,程进,宋强.MOCVD法制备一维氧化物阵列材料[J].北京航空航天大学学报,2004,30(10):939-943. 被引量：5
  • 3刘建刚,范新会,严文,于灵敏,刘春霞.热蒸发锌粉法制备半导体氧化锌纳米线的研究[J].材料科学与工程学报,2005,23(1):109-111. 被引量：19
  • 4陈庆春.D-山梨醇和n(OH^-)/n(Zn^(2+))对氧化锌形貌的影响[J].精细化工,2005,22(4):253-255. 被引量：6
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  • 10Sun X C,Zhang H Z,Xu J,et al.Shape controllable synthesis of ZnO nanorod arrays via vapor phase growth[J].Solid State Communications,2004,(129):803～807.

引证文献2

二级引证文献7

东北大学学报（自然科学版）
2005年 第11期

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