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苯丙胺类毒品五氟丙酰化气-质联用分析 被引量:2

GC -MC Analysis of Amphetamines after Derivation by Pentafluoropropionic Anhydride
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摘要 本文采用五氟丙酸酐(PFPA)衍生化试剂对苯丙胺类毒品进行衍生化,用气相色谱- 质谱法对衍生化产物进行测定;提供了衍生化产物经气~质联用分析后的总离子流色谱图、质谱 图及质谱断裂规律,以及一些定量参数。
作者 孟品佳
出处 《中国人民公安大学学报(自然科学版)》 2005年第4期4-6,共3页 Journal of People’s Public Security University of China(Science and Technology)
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  • 1[1]G. E. Platoff Jr, D. W. Hill, T. R. Koch and Y. H. Caplan.Serial capillary gas chromatography/fourier transform infrared spectrometry/mass spectrometry (GC/IR/MS): qualitative and quatitative analysis of amphetamine, methamphetamine, and related analogues in human urine. J Anal Toxi,16 (1992) 389~397.
  • 2[2]R. Meatherall. Rapid GC/MS confirmation of urinary amphetamine and methamphetamine as their propylchloroformate derivatives. J Anal Toxi, 19 (1995) 316 ~322.
  • 3[3]Valentine J. L. , Kearns G. L. , Sparks C. , Letzig L. G. ,Valentine C. R. , Shappell S. A. , Neri D. F. , and Dejohn C. A.. GC - MS determination of amphetamine and methamphetamine in human urine for 12 hours following oral administration of dextro - methamphetamine: lack of evidence supporting established forensic guidelines for methamphetamine confirmation. J Anal. Tox., 19 (1995) 581.
  • 4[4]Nobuyuki Nagasawa, Mikio Yashiki, Yasumasa Iwasaki,etc, Rapid analysis of amphetamines in blood using head space -solid phase microextraction and selected ion monitoring, Forensic Sci Int, 78 (1996) 95.

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