期刊文献+

淋洗液发生器离子色谱电导抑制法测定饮料中的添加剂 被引量:8

Determination of Food Additives in Beverages by Ion Chromatography
下载PDF
导出
摘要 建立了淋洗液发生器电导抑制离子色谱同时测定饮料中的阿斯巴甜、山梨酸、甜蜜素、苯甲酸、安赛蜜和糖精钠6种添加剂的方法,采用阴离子交换色谱柱IonPac AS11为分离柱,自动淋洗液发生器产生的高纯KOH梯度进行淋洗,饮料样品经稀释和0.2μm微孔滤膜过滤后,可直接进样分析。方法的线性范围广,灵敏度高,重现性好,简便,可用于饮料添加剂的分析。 An analytical method for simultaneous determination of six sweeteners and preserves in beverages including aspartame, sorbic acid, sodium cyclamate, benzoic acid, acesulfame K, sodium saccharine by suppressed ion chromatography has been developed.The anion column-IonPac AS l IHC column, and the eluent generator was used. Samples pretreated by dilution and filtration could be directly injected. The method enjoyed a wide linear range, good recoveries and high sensitivity. The results showed that the method was simple, accurate and might be good for analysis of food additives in beverages.
作者 曾爱民
出处 《现代科学仪器》 2005年第5期64-65,共2页 Modern Scientific Instruments
关键词 淋洗液发生器 离子色谱 甜味剂 防腐剂 Eluent generator ion chromatography sweetener preserves
  • 相关文献

参考文献4

二级参考文献7

  • 1PRODOLLIET J, BRUELHART M. Determination of aspartame and its major decomposition products in foods [J]. J AOAC, 1993, (76) :275-277.
  • 2ABOUL-ENEIN Y, BAKR S A. Comparative study of the separation and determination of aspartame and its decomposition products in bulk material and diet soft drinks by HPLC and CE H. Liq [J]. Chromatogra Catogr Rel Technol, 1997, (20): 1437-1440.
  • 3WROBEL K, WROBEL K. Determination of aspartame and phenylalanine in diet soft drinks by highperformance liquid chromatography with direct spectrofluorimetric detection [J]. J Chromtogr A, 1997,(773): 163-165.
  • 4CHEN Q C, MOU S F, LIU K N, et al. Separation and determination of four artificial sweeteners and citric acid by high-performance anion-exchange chromatography [J]. J Chromatogr A, 1997, (771): 135-140.
  • 5QU F,QI Z H, LIU K N, et al. Determination of aspartame by ion chromatography with electrochemical in tergrated amperometric detection [J]. J Chromatogr A,1999, (850): 277-279.
  • 6李明元,色谱,1988年,6卷,44页
  • 7A. M. Pietra,V. Cavrini,D. Bonazzi,L. Benfenati. HPLC analysis of aspartame and saccharin in pharmaceutical and dietary formulations[J] 1990,Chromatographia(3-4):215~219

共引文献48

同被引文献107

引证文献8

二级引证文献80

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部