摘要
对合成玉嘧磺隆文献进行了综述,提出了合理的合成路线,并运用固体光气合成玉嘧磺隆,产品纯度大于96%(HPLC法),总收率不小于36%。所有中间体及目标化合物的结构用1HNMR、IR及MS进行了表征。
The reasonable synthesis method of rimsulfuron was given based on summarization of literatures published. The intermediates were prepared and the title compound was synthesized by triphosgene at last. The purity of the product was over 96%（by HPLC）, and the total yield was not less than 36%. The structures of all compounds synthesized were determined by ^1HNMR, IR and MS.
出处
《农药》
CAS
北大核心
2005年第12期541-543,共3页
Agrochemicals
基金
2005年江苏省科技攻关(三药)项目(BE2005611)
