摘要
目的:建立救急行军散中雄黄的含量测定方法。方法:采用分光光度法对散剂中雄黄所含有的砷进行定量分析。结果:砷的线性范围为2.5-22.5 μg,r=0.9995,平均回收率为100.1%,RSD为1.0%。结论:方法简便可行、重线性好,适用于该制剂的质量控制。
Objective: To establish a method for determination of Realgar in Jiuji xingjun Powder, Method: to determine the arsenic in Realgar of Jiuji xingjun Powder was used by UV Spectrophotometry method. Result: The linear range was 2.5 -22.5 μg for arsenie( r = 0.999 5, n = 7 ), The average recovery was 100.1% and RSD was 1.0%. Conclusion: The method is simple, feasible and reproducible. It can be used for the quality control of Jiuji xingjun Powder.
出处
《中国药师》
CAS
2005年第12期1010-1010,1048,共2页
China Pharmacist
关键词
救急行军散
雄黄
砷
含量测定
Jiuji xingjun Powder
Realgar
Arsenic
Content