二乙酰基二茂铁二腙的合成

The Synthetic of Two Acetyl and Two Luxuriant Irons and Two Arbazone

用三氯甲烷作溶剂、三氯化铝作催化剂的条件下进行Friedel-Crafts酰基化反应,合成了1,1’-二乙 酰基二茂铁,其产率为55％．1,1’-二乙酰基二茂铁,在少量盐酸催化下用无水乙醇作溶剂,合成了二乙酰基二 茂铁二腙．

Make solvents with the chloroform, Three chlorine aluminium reglect friedel - Crafts aeyl base under the terms to make catalyst. Formate 1,1＇- two acetyl 2 luxuriant iron, Its producing rate is 55%. 1,1 ＇ - two acetyl two luxuriant iron, hydrazine make solvents with the anhydrous ethanlol under the hydroger catalysis in a small amount of chlorine , formate one two luxuriant two acetyl and two luxuriant iron and two ambazone of complexing material of iron.