摘要
研究了利用N-乙酰-L-谷氨酸为拆分试剂,成功的对氯化3-氰-2-羟丙基三甲胺进行光学拆分,一次拆分光学纯度为92%,产率为37%;二次拆分光学纯度达95%,产率为29.1%。
Optical resolution of the 3 - cyano - 2 - hydroxypropyl trithylamamin chloride using N - acetyl - L - glutamic acid as resolution agent was studied. Optical purity of resolution of L - 3 - cyano - 2 - hydroxypropyl trimethylamin chloride was 92%. The yield was 37%. Optical purity of its secondry purity was 95%. They yield was 29.1%.
出处
《南昌大学学报(理科版)》
CAS
北大核心
2005年第6期526-528,532,共4页
Journal of Nanchang University(Natural Science)
基金
江西省科技厅2000年工业攻关项目(Z-01707)