摘要
在乙醚和95%乙醇溶剂中,以过碳酸钠为助氧化剂,通入空气,将苯硒酚制成二苯二硒,收率可达76.5%(以溴苯计)。
This paper reports our results concerning the improved synthesis of diphenyldiselenide by oxidation of selenophenol with atmospheric oxygen in the presence of sodium percarbonate,ether and 95 % ethanol. The yield of the product is 76.5%(based on brombenzene).
出处
《精细化工》
CAS
CSCD
1996年第3期27-28,共2页
Fine Chemicals
关键词
二苯二硒
苯硒酚
合成
试剂
Diphenyldiselenide,Selenophenol,Synthesis