摘要
基于在浓盐酸介质中，二价铅离子所形成的PbCl4^2-在紫外光的照射下发蓝色荧光的原理，建立利用荧光测水样中微量铅的方法。该方法线性范围为0．03-2．00μg/m，检出限为9．1×10^-3μg／mL，用于水样中微量铅的测定，加标回收率为92．8％-100．3％。
Pb^2＋ in concentrated HCl solution formed PbCI4^2- and showed fluorescence after being excited by UV. Based on this, a Fluofimetrie method for determination of trace lead in water samples was established .The line range for the determination of lead was 0.03 - 2.00 μg/mL, with the determination limit of 9.1 × 10^-3μg/mL. The method was applied to determine micro lead in water samples, the recovery was 92.8 % - 100.3 % .
出处
《辽宁化工》
CAS
2006年第2期121-122,124,共3页
Liaoning Chemical Industry
关键词
荧光分析法
水
铅氯配合物
Fluorimelric method
Water samples
PbCl4^2-
