摘要
以β-萘胺和甘油为原料,利用斯克柔普(Skraup)法合成了4-氮杂菲,并进行了对比试验,当重量比为β-萘胺:甘油:浓硫酸:冰乙酸:脱氢剂=1:1.74:1.75:0.58:0.84时,收率最高。
With β-naphthylamine and glycerin as the raw material, 4-azaphenanthrine was synthesized by Skraup method,and contrast experiment was carried out on it. If the ratio of weight is β-naphthylam-ine： glycerin： concentrated sulfuric acid： glacial acetic acid： dehydrogenated agent=1：1.74：1.75：0.58：0.84, the yield is the highest.
出处
《江苏技术师范学院学报》
2005年第6期68-69,40,共3页
Journal of Jiangsu Teachers University of Technology
关键词
4-氯杂菲
β-萘胺
合成
4-azaphenanthrine
β-naphthylamine
synthesis
